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Research Article

Ultrathin Zn-free anode based on Ti3C2Tx and nanocellulose enabling high-durability aqueous hybrid Zn-Na battery with Zn2+/Na+ co-intercalation mechanism

Hao Chen1, Weijun Zhou1, Minfeng Chen1, Qinghua Tian2, Xiang Han1,3, Jizhang Chen1,3( )
College of Materials Science and Engineering, Nanjing Forestry University, Nanjing 210037, China
Key Laboratory of Surface & Interface Science of Polymer Materials of Zhejiang Province, Department of Chemistry, Zhejiang Sci-Tech University, Hangzhou 310018, China
Co-Innovation Center of Efficient Processing and Utilization of Forest Resources, Nanjing Forestry University, Nanjing 210037, China
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Graphical Abstract

Layer-by-layer deposited β-In2Se3 from 1 to 13 L on monolayer MoS2 forms vertical β-In2Se3/MoS2 heterostructures. Attributed to abundant layer-dependent edge active sites, edge reconstruction, improved hydrophilicity and high electrical conductivity of β-In2Se3/MoS2 heterostructures, excellent electrocatalytic hydrogen evolution performance with lower onset potential (77.3 mV) and smaller Tafel slope (47.1 mV·dec–1) can be observed at the edge of monolayer MoS2 coupled with 13-L β-In2Se3.

Abstract

With low cost and high safety, aqueous zinc-based batteries have received considerable interest. Nevertheless, the excess utilization of zinc metal in the anodes of these batteries reduces energy density and increases costs. Herein, an ultrathin electrode of approximately 6.2 μm thick is constructed by coating Ti3C2Tx/nanocellulose hybrid onto a stainless steel foil. This electrode is used as the Zn-free anode for aqueous hybrid Zn-Na battery, in which, a concentrated electrolyte is used to improve electrochemical reversibility. The Ti3C2Tx/nanocellulose coating is found to improve the electrolyte wettability, facilitate desolvation process of hydrated Zn2+ ions, lower nucleation overpotential, improve zinc plating kinetics, guide horizontal zinc plating along the Zn(002) facet, and inhibit parasitic side reactions. It is also found that the Na3V2(PO4)3 cathode material adopts a highly reversible Zn2+/Na+ co-intercalation charge storage mechanism in this system. Thanks to these benefits, the assembled hybrid Zn-Na battery exhibits excellent rate capability, superior cyclability, and good anti-freezing ability. This work provides a new concept of electrode design for electrochemical energy storage.

Keywords

MXene-based compositesultrathin electrodeselectrode surface coatingsaqueous hybrid batteriesco-intercalation charge storage mechanisms

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Nano Research
Volume 16 Issue 1,
January 2023
Pages 536-544
DOI: 10.1007/s12274-022-4916-z
Cite this article:
Chen H, Zhou W, Chen M, et al. Ultrathin Zn-free anode based on Ti3C2Tx and nanocellulose enabling high-durability aqueous hybrid Zn-Na battery with Zn2+/Na+ co-intercalation mechanism. Nano Research, 2023, 16(1): 536-544. https://doi.org/10.1007/s12274-022-4916-z
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Received: 21 June 2022
Revised: 28 July 2022
Accepted: 15 August 2022
Published: 03 September 2022
© Tsinghua University Press 2022
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