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Research Article

Boosted microwave absorption performance of transition metal doped TiN fibers at elevated temperature

Cuiping Li1,2,§, Dan Li1,2,§, Lu Zhang1,2, Yahong Zhang3, Lei Zhang1,2, Chunhong Gong1,2( ), Jingwei Zhang2
Institute of Functional Polymer Composites, College of Chemistry and Chemical Engineering, Henan University, Kaifeng 475004, China
National & Local Joint Engineering Research Center for Applied Technology of Hybrid Nanomaterials, Henan University, Kaifeng 475004, China
Key Laboratory of Micro-Nano Materials for Energy Storage and Conversion of Henan Province, Institute of Surface Micro and Nano Materials, College of Chemical and Materials Engineering, Xuchang University, Xuchang 461000, China

§ Cuiping Li and Dan Li contributed equally to this work.

Show Author Information

Graphical Abstract

The transition metal-doped titanium nitride (M-TiN, M = Fe or Co) is fracibated and can produce defects, heterointerfaces, and more charge accumulation attributed to the transition metal-doping, which affect the polarization loss and conduction loss, further lead to enhancement of dielectric response and electromagnetic wave absorption (EMWA) performances. Due to the negative correlation between polarization loss and temperature, the optimization of EMWA performances in wide temperature domain could be realized by introducing appropriate polarization loss and its compensating.

Abstract

Due to the temperature and frequency response of electromagnetic (EM) loss, how to realize the effective design of microwave absorption materials (MWAMs) at elevated temperature is highly desirable for practical applications. Herein, transition metal-doped titanium nitride (M-TiN, M = Fe or Co) fibers were fabricated, the distortion of TiN lattice could cause the adjustable charge enrichment, which played a profound influence on the dielectric response and EM microwave absorption (EMWA) performances. Benefiting from the negative correlation between dielectric loss and temperature, more loss mechanism could be introduced, which would effectively enhance dielectric loss and EMWA performances at elevated temperature. The optimal EMWA performances of Fe-TiN fibers/polydimethylsiloxane (PDMS) composites were realized with a wide temperature range (298–423 K): the reflection loss (RL) could reach 99% (RL < −20 dB) at 12.2 GHz with 1.8 mm, when the filler content was only 15.0 wt.%. Compared with the undoped-TiN fibers/PDMS and Co-TiN fibers/PDMS composites, the excellent EMWA of Fe-TiN fibers/PDMS composite could be attributed to the reasonably synergistic polarization loss and conduction loss. Based on systematic analysis of the variable-temperature EM parameters and EMWA performances, the optimization of EMWA performances in wide temperature domain could be realized by introducing appropriate polarization loss and its compensating. Hopefully, this work provides a new strategy for regulating the dielectric response and designing effective MWAMs at elevated temperature.

Keywords

transition metal-doped TiNpolarization lossdielectric responseelectromagnetic microwave absorption

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Nano Research
Volume 16 Issue 2,
February 2023
Pages 3570-3579
DOI: 10.1007/s12274-023-5398-3
Cite this article:
Li C, Li D, Zhang L, et al. Boosted microwave absorption performance of transition metal doped TiN fibers at elevated temperature. Nano Research, 2023, 16(2): 3570-3579. https://doi.org/10.1007/s12274-023-5398-3
Topics:
Metal ions
Part of a topical collection:
EM Wave Functional Materials

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Received: 21 November 2022
Revised: 06 December 2022
Accepted: 08 December 2022
Published: 31 December 2022
© Tsinghua University Press 2023
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