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Research Article

Optimizing electronic structure of NiFe LDH with Mn-doping and Fe0.64Ni0.36 alloy for alkaline water oxidation under industrial current density

Yang Qian1, Fan Zhang1, Lingshu Qiu1, Weiwei Han1, Zixu Zeng1, Lecheng Lei1,2, Yi He1, Ping Li2, Xingwang Zhang1,2( )
Key Laboratory of Biomass Chemical Engineering of Ministry of Education, College of Chemical and Biological Engineering, Zhejiang University, Hangzhou 310027, China
Institute of Zhejiang University-Quzhou, Quzhou 324000, China
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Graphical Abstract

A series of in situ grown Mn-NiFe lactate dehydrogenase (LDH) nanosheet arrays were fabricated on the Fe0.64Ni0.36/NM (nickel mesh) alloy layer. Optimization of the electronic structure induced by Mn doping and the alloy layer introduction led to enhanced oxygen evolution reaction (OER) activity (η500 = 295 mV) and remarkable stability of Mn0.15-NiFe LDH/Fe0.64Ni0.36/NM.

Abstract

Alkaline electrolyzers for water splitting under the industrial current densities are always burdened with huge energy consumption due to the high overpotential and poor stability of the anode nanocatalysts for oxygen evolution reaction (OER). Inspired by the interfacial charge transfer for enhancing the performance, a series of in-situ grown interfacial Mn-NiFe lactate dehydrogenase (LDH) was designed on the Fe0.64Ni0.36/NM (nickel mesh) alloy layer. The optimized Mn0.15-NiFe LDH/Fe0.64Ni0.36/NM exhibited an ultralow overpotential of 295 mV to drive 500 mA·cm−2 and an incredible stability under large current density. The interfacial space and heteroatom doping synergistically triggered the electronic structure optimization to promote electron transfer and ensure the durability of the high-current reaction. Notably, the designed Mn0.15-NiFe LDH/Fe0.64Ni0.36/NM as an anode in an integral alkaline electrolyzer exhibited a cell voltage of 1.78 V at 500 mA·cm−2 with a stability of 366 h. Density functional theory (DFT) calculations further demonstrated the synergistic effect of alloy layer introduction and Mn doping could accelerate electron transfer and stabilize the charged active center to activate the NiFe LDH and reduce the OER energy barrier. Our work offers new insights into developing efficient self-supported catalysts for high-current alkaline water oxidation.

Keywords

heteroatom dopingalloy layer introductionsynergistic effecthigh-current alkaline water oxidation

Electronic Supplementary Material

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Nano Research
Volume 16 Issue 7,
July 2023
Pages 8953-8960
DOI: 10.1007/s12274-023-5615-0
Cite this article:
Qian Y, Zhang F, Qiu L, et al. Optimizing electronic structure of NiFe LDH with Mn-doping and Fe0.64Ni0.36 alloy for alkaline water oxidation under industrial current density. Nano Research, 2023, 16(7): 8953-8960. https://doi.org/10.1007/s12274-023-5615-0
Topics:
Nanocatalysts

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Received: 30 December 2022
Revised: 15 February 2023
Accepted: 23 February 2023
Published: 15 April 2023
© Tsinghua University Press 2023
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