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Research Article | Open Access

Enhanced thermal shock and oxidation resistance of Si2BC3N ceramics through MWCNTs incorporation

Ning LIAOa,b,c,d( ), Dechang JIAa,b( ), Zhihua YANGa,b, Yu ZHOUa,b, Yawei LIc,d
Institute for Advanced Ceramics, School of Materials Science and Engineering, Harbin Institute of Technology, Harbin 150080, China
Key Laboratory of Advanced Structure-Function Integrated Materials and Green Manufacturing Technology, Ministry of Industry and Information Technology, China
State Key Laboratory of Refractories and Metallurgy, Wuhan University of Science and Technology, Wuhan 430081, China
National–provincial Joint Engineering Research Center of High Temperature Materials and Lining Technology, Wuhan, China
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Abstract

Multi-walled carbon nanotubes (MWCNTs) reinforced Si2BC3N ceramics were prepared through mechanical alloying (MA) and following spark plasma sintering (SPS). The thermal shock resistance of Si2BC3N ceramics was evaluated comparatively through ice water quenching test and theoretical prediction. Furthermore, the oxidation resistance of MWCNTs incorporated Si2BC3N ceramics was evaluated under high temperature. The results show that the calculated parameters such as the critical thermal shock temperature (R) and the thermal stresses resistance (Rst), as well as the toughness (R′′′′) are improved with addition of 1 vol% MWCNTs. In addition, the crack propagation resistance of 1 vol% MWCNTs incorporated Si2BC3N ceramics is obviously improved through generating more tortuous crack propagation paths attributing to the “crack bridging”, “pull-out”, and “crack deflection” mechanisms of MWCNTs. Therefore, the residual strengths of 1 vol% MWCNTs containing specimens remained the highest after the thermal shock tests. Besides, the present work also reveals that the oxidation resistance is more sensitive to relative density than MWCNTs addition.

Keywords

Si2BC3N ceramicsMWCNTsthermal shock resistanceoxidation resistance

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Journal of Advanced Ceramics
Volume 7 Issue 3,
September 2018
Pages 276-288
DOI: 10.1007/s40145-018-0279-z
Cite this article:
LIAO N, JIA D, YANG Z, et al. Enhanced thermal shock and oxidation resistance of Si2BC3N ceramics through MWCNTs incorporation. Journal of Advanced Ceramics, 2018, 7(3): 276-288. https://doi.org/10.1007/s40145-018-0279-z

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Received: 25 February 2018
Revised: 25 April 2018
Accepted: 27 April 2018
Published: 10 October 2018
© The author(s) 2018

Open Access The articles published in this journal are distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution, and reproduction in any medium, provided you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made.
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