AI Chat Paper
Note: Please note that the following content is generated by AMiner AI. SciOpen does not take any responsibility related to this content.
{{lang === 'zh_CN' ? '文章概述' : 'Summary'}}
{{lang === 'en_US' ? '中' : 'Eng'}}
Chat more with AI
Powered by AMiner. Clicking this button will take you away from SciOpen.
Home Journal of Advanced Ceramics Article
PDF (3.7 MB)
Cite
EndNote(RIS) BibTeX
Collect
Submit Manuscript AI Chat Paper
Show Outline
Outline
Show full outline
Hide outline
Outline
Show full outline
Hide outline
Research Article | Open Access

Ablation of C/SiC-HfC composite prepared by precursor infiltration and pyrolysis in plasma wind tunnel

Liuyang DUANa, Lei LUOb, Liping LIUa,c, Yiguang WANGd( )
Science and Technology on Thermostructural Composite Materials Laboratory, Northwestern Polytechnical University, Xi’an 710072, China
Beijing Institute of Long March Aerospace Vehicles, Beijing 100076, China
Ultrahigh Speed Aerodynamics Research Institute, China Aerodynamics Research and Development Center, Mianyang 621000, China
Institute of Advanced Structure Technology, Beijing Institute of Technology, Haidian District, Beijing 100081, China
Show Author Information

Abstract

Carbon fiber reinforced silicon carbide-hafnium carbide (C/SiC-HfC) composite was prepared by precursor infiltration and pyrolysis process. Then, ablation behavior of C/SiC-HfC was evaluated in plasma wind tunnel. It was found that oxide layer formed during ablation significantly influenced the surface temperature. Formation of dense HfO2-SiO2 layer under low heat flux led to stable surface temperature. Silica (SiO2) on the surface was gradually consumed when heat flux increased, resulting in conversion of HfO2-SiO2 on the surface to HfO2. Converted HfO2 with high catalytic coefficient absorbed more energy, causing gradual increase in the surface temperature. Formed oxide layer was destroyed at high heat flux and high stagnation point pressure. After carbon fiber lost the protection of HfO2-SiO2 layer, it burned immediately, leading to surface temperature jump.

Keywords

C/SiC-HfC compositeprecursor infiltration and pyrolysisablationplasma wind tunnel

References

[1]
TH Squire, J Marschall. Material property requirements for analysis and design of UHTC components in hypersonic applications. J Eur Ceram Soc 2010, 30: 2239-2251.
Crossref Google Scholar
[2]
DE Glass. Ceramic matrix composite (CMC) thermal protection systems (TPS) and hot structures for hypersonic vehicles. In: Proceedings of the 15th AIAA International Space Planes and Hypersonic Systems and Technologies Conference, 2008: AIAA-2008-2682.
Crossref
[3]
QS Ma, LH Cai. Fabrication and oxidation resistance of mullite/yttrium silicate multilayer coatings on C/SiC composites. J Adv Ceram 2017, 6: 360-367.
Crossref Google Scholar
[4]
YD Xu, LT Zhang, LF Cheng, et al. Microstructure and mechanical properties of three-dimensional carbon/silicon carbide composites fabricated by chemical vapor infiltration. Carbon 1998, 36: 1051-1056.
Crossref Google Scholar
[5]
W Krenkel, F Berndt. C/C-SiC composites for space applications and advanced friction systems. Mat Sci Eng A 2005, 412: 177-181.
Crossref Google Scholar
[6]
I Sakraker, CO Asma. Experimental investigation of passive/active oxidation behavior of SiC based ceramic thermal protection materials exposed to high enthalpy plasma. J Eur Ceram Soc 2013, 33: 351-359.
Crossref Google Scholar
[7]
MJH Balat. Determination of the active-to-passive transition in the oxidation of silicon carbide in standard and microwave-excited air. J Eur Ceram Soc 1996, 16: 55-62.
Crossref Google Scholar
[8]
WL Vaughn, HG Maahs. Active-to-passive transition in the oxidation of silicon carbide and silicon nitride in air. J Am Ceram Soc 1990, 73: 1540-1543.
Crossref Google Scholar
[9]
MM Opeka, IG Talmy, JA Zaykoski. Oxidation-based materials selection for 2000 °C + hypersonic aerosurfaces: Theoretical considerations and historical experience. J Mater Sci 2004, 39: 5887-5904.
Crossref Google Scholar
[10]
Y Arai, R Inoue, K Goto, et al. Carbon fiber reinforced ultra-high temperature ceramic matrix composites: A review. Ceram Int 2019, 45: 14481-14489.
Crossref Google Scholar
[11]
X Zhao, YG Wang, LY Duan, et al. Improved ablation resistance of C/SiC-ZrB2 composites via polymer precursor impregnation and pyrolysis. Ceram Int 2017, 43: 12480-12489.
Crossref Google Scholar
[12]
KX Gui, FY Liu, G Wang, et al. Microstructural evolution and performance of carbon fiber-toughened ZrB2 ceramics with SiC or ZrSi2 additive. J Adv Ceram 2018, 7: 343-351.
Crossref Google Scholar
[13]
ZJ Yu, X Lv, SY Lai, et al. ZrC-ZrB2-SiC ceramic nanocomposites derived from a novel single-source precursor with high ceramic yield. J Adv Ceram 2019, 8: 112-120.
Crossref Google Scholar
[14]
YT Chen, W Sun, X Xiong, et al. Microstructure, thermophysical properties, and ablation resistance of C/HfC-ZrC-SiC composites. Ceram Int 2019, 45: 4685-4691.
Crossref Google Scholar
[15]
J Chen, YG Wang, LF Cheng, et al. Thermal diffusivity of three-dimensional needled C/SiC-TaC composites. Ceram Int 2011, 37: 3095-3099.
Crossref Google Scholar
[16]
QB Wen, R Riedel, E Ionescu. Solid-solution effects on the high-temperature oxidation behavior of polymer-derived (Hf, Ta)C/SiC and (Hf, Ti)C/SiC ceramic nanocomposites. Adv Eng Mater 2019, 21: 1800879.
Crossref Google Scholar
[17]
JP Zhang, JL Qu, QG Fu. Ablation behavior of nose-shaped HfB2-SiC modified carbon/carbon composites exposed to oxyacetylene torch. Corros Sci 2019, 151: 87-96.
Crossref Google Scholar
[18]
SQ Guo, K Naito, Y Kagawa. Mechanical and physical behaviors of short pitch-based carbon fiber-reinforced HfB2-SiC matrix composites. Ceram Int 2013, 39: 1567-1574.
Crossref Google Scholar
[19]
YT Chen, W Sun, X Xiong, et al. Microstructure, thermophysical properties, and ablation resistance of C/HfC-ZrC-SiC composites. Ceram Int 2019, 45: 4685-4691.
Crossref Google Scholar
[20]
L Luo, YG Wang, LY Duan, et al. Ablation behavior of C/SiC-HfC composites in the plasma wind tunnel. J Eur Ceram Soc 2016, 36: 3801-3807.
Crossref Google Scholar
[21]
VC Agte, H Altertum. Untersuchungen über systeme hochschmelzender carbide nebst beitr ägen zum problem der kohlenstoffschmelzung. Z Tech Physik 1930, 11: 182.
Google Scholar
[22]
SM Lakiza, JS Tyschenko, LM Lopato. Phase diagram of the Al2O3-HfO2-Y2O3 system. J Eur Ceram Soc 2011, 31: 1285-1291.
Crossref Google Scholar
[23]
D Huang, MY Zhang, QZ Huang, et al. Mechanical property, oxidation and ablation resistance of C/C-ZrB2- ZrC-SiC composite fabricated by polymer infiltration and pyrolysis with preform of Cf/ZrB2. J Mater Sci Technol 2017, 33: 481-486.
Crossref Google Scholar
[24]
CL Yan, RJ Liu, CR Zhang, et al. Ablation and mechanical properties of 3D braided C/ZrC-SiC composites with various SiC/ZrC ratios. Ceram Int 2016, 42: 19019-19026.
Crossref Google Scholar
[25]
LY Duan, X Zhao, YG Wang. Comparative ablation behaviors of C/SiC-HfC composites prepared by reactive melt infiltration and precursor infiltration and pyrolysis routes. Ceram Int 2017, 43: 16114-16120.
Crossref Google Scholar
[26]
HB Fan, NK Ravala, HC Wikle III, et al. HfC structural foams synthesizing from polymer precursors. In: Innovative Processing and Synthesis of Ceramics, Glasses and Composites IX. NP Singh, BG Bansal, T Nair, et al. Eds. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2012: 13-24.
Crossref
[27]
QB Wen, XG Luan, L Wang, et al. Laser ablation behavior of SiHfC-based ceramics prepared from a single-source precursor: Effects of Hf-incorporation into SiC. J Eur Ceram Soc 2019, 39: 2018-2027.
Crossref Google Scholar
[28]
DVN Harish, A Bharatish, HNN Murthy, et al. Evaluation of nanosecond laser ablation and scratch resistance of tantalum carbide coated graphite substrates. Ceram Int 2019, 45: 22578-22588.
Crossref Google Scholar
[29]
A Nisar, S Ariharan, T Venkateswaran, et al. Effect of carbon nanotube on processing, microstructural, mechanical and ablation behavior of ZrB2-20SiC based ultra-high temperature ceramic composites. Carbon 2017, 111: 269-282.
Crossref Google Scholar
[30]
S Mungiguerra, GD di Martino, A Cecere, et al. Arc-jet wind tunnel characterization of ultra-high-temperature ceramic matrix composites. Corros Sci 2019, 149: 18-28.
Crossref Google Scholar
[31]
F Panerai, B Helber, O Chazot, et al. Surface temperature jump beyond active oxidation of carbon/silicon carbide composites in extreme aerothermal conditions. Carbon 2014, 71: 102-119.
Crossref Google Scholar
[32]
M Auweter-Kurtz, HL Kurtz, S Laure. Plasma generators for re-entry simulation. J Propul Power 1996, 12: 1053-1061.
Crossref Google Scholar
[33]
F Monteverde, R Savino, M de Stefano Fumo, et al. Plasma wind tunnel testing of ultra-high temperature ZrB2-SiC composites under hypersonic re-entry conditions. J Eur Ceram Soc 2010, 30: 2313-2321.
Crossref Google Scholar
[34]
F Monteverde, R Savino, M de Stefano Fumo. Dynamic oxidation of ultra-high temperature ZrB2-SiC under high enthalpy supersonic flows. Corros Sci 2011, 53: 922-929.
Crossref Google Scholar
[35]
P Lespade, N Richet, P Goursat. Oxidation resistance of HfB2-SiC composites for protection of carbon-based materials. Acta Astronaut 2007, 60: 858-864.
Crossref Google Scholar
[36]
YG Wang, BS Ma, LL Li, et al. Oxidation behavior of ZrB2-SiC-TaC ceramics. J Am Ceram Soc 2012, 95: 374-378.
Crossref Google Scholar
[37]
L Luo, YG Wang, LP Liu, et al. Ablation behavior of C/SiC composites in plasma wind tunnel. Carbon 2016, 103: 73-83.
Crossref Google Scholar
[38]
T Grau, E Messerschmid. Numerical investigation of a partially ionized air flow in a plasma wind tunnel. In: Proceedings of the 7th AIAA/ASME Joint Thermophysics and Heat Transfer Conference, 1998: AIAA-98-2955.
Crossref
[39]
D Alfano, L Scatteia, S Cantoni, et al. Emissivity and catalycity measurements on SiC-coated carbon fibre reinforced silicon carbide composite. J Eur Ceram Soc 2009, 29: 2045-2051.
Crossref Google Scholar
[40]
GR Holcomb. Countercurrent gaseous diffusion model of oxidation through a porous coating. Corrosion 1996, 52: 531-539.
Crossref Google Scholar
[41]
F Yang, JM Gu, LH Ye, et al. Justifying the significance of Knudsen diffusion in solid oxide fuel cells. Energy 2016, 95: 242-246.
Crossref Google Scholar
[42]
R Savino, M de Stefano Fumo, L Silvestroni, et al. Arc-jet testing on HfB2 and HfC-based ultra-high temperature ceramic materials. J Eur Ceram Soc 2008, 28: 1899-1907.
Crossref Google Scholar
[43]
S Caniglia, GL Barna. Handbook of Industrial Refractories Technology: Principles, Types, Properties and Applications. William Andrew, 1992: 135.
[44]
B Helber, O Chazot, A Hubin, et al. Microstructure and gas-surface interaction studies of a low-density carbon-bonded carbon fiber composite in atmospheric entry plasmas. Compos Part A: Appl S 2015, 72: 96-107.
Crossref Google Scholar
[45]
M Gasch, D Ellerby, E Irby, et al. Processing, properties and arc jet oxidation of hafnium diboride/silicon carbide ultra high temperature ceramics. J Mater Sci 2004, 39: 5925-5937.
Crossref Google Scholar
Journal of Advanced Ceramics
Volume 9 Issue 3,
June 2020
Pages 393-402
DOI: 10.1007/s40145-020-0379-4
Cite this article:
DUAN L, LUO L, LIU L, et al. Ablation of C/SiC-HfC composite prepared by precursor infiltration and pyrolysis in plasma wind tunnel. Journal of Advanced Ceramics, 2020, 9(3): 393-402. https://doi.org/10.1007/s40145-020-0379-4

1008

Views

118

Downloads

69

Crossref

N/A

Web of Science

70

Scopus

12

CSCD

Altmetrics
Received: 23 December 2019
Revised: 14 March 2020
Accepted: 31 March 2020
Published: 05 June 2020
© The Author(s) 2020

This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if changes were made.

The images or other third party material in this article are included in the article’s Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder.

To view a copy of this licence, visit http://creativecommons.org/licenses/by/4.0/.
Return