PDF (1.9 MB)
Collect
Submit Manuscript
Show Outline
Outline
Abstract
Keywords
References
Show full outline
Hide outline
Publishing Language: Chinese

Wettability and its major determinants of shale reservoirs in the Shahejie Formation, Dongying Sag, Bohai Bay Basin

Qianwen LI1,2,3()
State Key Laboratory of Shale Oil and Gas Enrichment Mechanisms and Effective Development, Beijing 102206, China
Key Laboratory of Shale Oil/Gas Exploration and Production Technology, SINOPEC, Beijing 102206, China
Petroleum Exploration and Production Research Institute, SINOPEC, Beijing 100026, China
Show Author Information

Abstract

Wettability, a factor influencing the occurrence and seepage patterns of shale oil in reservoirs, is an important indicator of shale reservoir evaluation. Using contact angle measurements and spontaneous imbibition experiments, we quantitatively characterize the wettability of shale reservoirs in the Shahejie Formation, Dongying Sag, Bohai Bay Basin, while delving into the primary determinants of wettability, and selecting the optimal reservoirs for assessment. The findings suggest that the shale reservoirs in the Shahejie Formation exhibit moderate pore connectivity and fractional wettability, generally proving to be water-wet to weakly water-wet. The reservoir wettability is jointly determined by organic matter characteristics, mineral components, pore size, and shale oil composition. The impacts of organic matter and mineral composition on reservoir wettability depend on the interfacial tension of solid particles. Specifically, a higher abundance of organic matter and a higher calcium content in minerals are associated with reduced water wettability and stronger oil wettability of the reservoirs. The oil-bearing capacity and shale oil components alter the surface tension of liquids, further influencing the reservoir wettability. A higher oil-bearing capacity of reservoirs and the presence of more polar components in crude oil suggest stronger oil wettability. Pore structure influences the solidliquid interfacial tension through capillary pressure, further affecting the reservoir wettability. A larger pore sizecorresponds to weaker water wettability and stronger oil wettability of the reservoirs. The wettability assessment results demonstrate that lamellar organic-rich calcareous shales exhibit the strongest lipophilicity. Shale oil tends to be enriched and accumulate in these shales under weakly water-wet conditions, creating conducive conditions for shale oil production. Therefore, these shales serve as favorable targets for shale oil exploration and production.

CLC number: TE122.2 Document code: A Article ID: 0253-9985(2024)04-1142-13

References

[1]

WANG Min, MA Rui, LI Jinbu, et al. Occurrence mechanism of lacustrine shale oil in the Paleogene Shahejie Formation of Jiyang Depression, Bohai Bay Basin, China[J]. Petroleum Exploration and Development, 2019, 46(4): 789-802.

[2]

DAI Jinyou, LIN Lixin. “Seepage” classification scheme of reservoir pores and its significance[J]. Petroleum Geology & Oilfield Development in Daqing, 2022, 41(2): 43-50.

[3]

XU Tianwu, ZHANG Chengfu, LI Honglei, et al. Research on lower limits of key factor controlling hydrocarbon accumulation of continental shale in different environments: Taking exploratory area of Zhongyuan Oilfield as an example[J]. Fault-Block Oil and Gas Field, 2022, 29(6): 721-728, 743.

[4]

LI Qianwen, LIU Zhongbao, CHEN Feiran, et al. Behavior and controlling factors of methane adsorption in Jurassic continental shale, northeastern Sichuan Basin[J]. Energy Geoscience, 2023, 4(1): 83-92.

[5]

ZHENG Guowei, GAO Zhiye, HUANG Liliang, et al. Wettability of the Permian Fengcheng formation shale in the Mahu Sag, Junggar Basin, and its main control factors[J]. Oil & Gas Geology, 2022, 43(5): 1206-1220.

[6]

ANDERSON W G. Wettability literature survey-part 1: Rock/oil/brine interactions and the effects of core handling on wettability[J]. Journal of Petroleum Technology, 1986, 38(10): 1125-1144.

[7]

HE Gengsheng, TANG Hai. Petrophysics[M]. 2nd ed. Beijing: Petroleum Industry Press, 2011: 240-242.

[8]

HU Qinhong, LIU Huimin, LI Maowen, et al. Wettability, pore connectivity and fluid-tracer migration in shale oil reservoirs of Paleogene Shahejie Formation in Dongying Sag of Bohai Bay Basin, East China[J]. Acta Petrolei Sinica, 2018, 39(3): 278-289.

[9]

WANG Xiaoming, CHEN Junbin, REN Dazhong. Research progress and prospect of pore structure representation and seepage law of continental shale oil reservoir[J]. Petroleum Reservoir Evaluation and Development, 2023, 13(1): 23-30.

[10]

FAN Yuchen, CHEN Lei, LIU Keyu, et al. Effects of wettability and pore water occurrence of gas storage space of shale reservoirs[J]. Journal of Central South University (Science and Technology), 2022, 53(9): 3575-3589.

[11]

MOSS A K, JING Xd, ARCHER J S. Laboratory investigation of wettability and hysteresis effects on resistivity index and capillary pressure characteristics[J]. Journal of Petroleum Science and Engineering, 1999, 24(2/4): 231-242.

[12]

LIU Xiangjun, XIONG Jian, LIANG Lixi, et al. Analysis of the wettability of Longmaxi Formation shale in the south region of Sichuan Basin and its influence[J]. Natural Gas Geoscience, 2014, 25(10): 1644-1652.

[13]

HU Qinhong, EWING R P, ROWE H D. Low nanopore connectivity limits gas production in Barnett formation[J]. Journal of Geophysical Research: Solid Earth, 2015, 120(12): 8073-8087.

[14]

XU M, DEHGHANPOUR H. Advances in understanding wettability of gas shales[J]. Energy & Fuels, 2014, 28(7): 4362-4375.

[15]

GAO Zhiye, HU Qinhong. Wettability of Mississippian Barnett Shale samples at different depths: Investigations from directional spontaneous imbibition[J]. AAPG Bulletin, 2016, 100(1): 101-114.

[16]

ARIF M, ZHANG Yihuai, IGLAUER S. Shale wettability: Data sets, challenges, and outlook[J]. Energy & Fuels, 2021, 35(4): 2965-2980.

[17]

SIDDIQUI M A Q, ALI S, FEI Haoxiang, et al. Current understanding of shale wettability: A review on contact angle measurements[J]. Earth-Science Reviews, 2018, 181: 1-11.

[18]

CLARKSON C R, JENSEN J L, PEDERSEN P K, et al. Innovative methods for flow-unit and pore-structure analyses in a tight siltstone and shale gas reservoir[J]. AAPG Bulletin, 2012, 96(2): 355-374.

[19]

ZENG Juan, YI Minghua, NIE Jun, et al. Research of quantitative characterization based on shale wet-ability in southeast Chongqing area[J]. Unconventional Oil & Gas, 2021, 8(1): 90-94.

[20]
LIU Xuan. Main factors controlling the wettability of shales[D]. Beijing: China University of Geosciences (Beijing), 2018.
[21]

ZHOU Lihong, HAN Guomeng, YANG Fei, et al. Geological characteristics and shale oil exploration of Es3(1) in Qikou Sag, Bohai Bay Basin[J]. Oil & Gas Geology, 2021, 42(2): 443-455.

[22]

LIU Huimin, LI Junliang, LIU Peng, et al. Enrichment conditions and strategic exploration direction of Paleogene shale oil in Jiyang Depression[J]. Acta Petrolei Sinica, 2022, 43(12): 1717-1729.

[23]

LAI Fuqiang, LI Shichao, WANG Min, et al. Optimal retrieval method for mineral constituents of shale oil reservoirs in Jiyang Sag[J]. Special Oil & Gas Reservoirs, 2022, 29(2): 16-23.

[24]

GUO Jianchun, TAO Liang, CHEN Chi, et al. A new method for evaluating the mixed wettability of shale in Longmaxi Formation in the southern Sichuan[J]. Acta Petrolei Sinica, 2020, 41(2): 216-225.

[25]

XIAO Wenlian, YANG Yubin, HUANG Chu, et al. Rock wettability and its influence on crude oil producing characteristics based on NMR technology[J]. Petroleum Geology and Recovery Efficiency, 2023, 30(1): 112-121.

[26]

ZHANG Linye, BAO Youshu, LI Juyuan, et al. Movability of lacustrine shale oil: A case study of Dongying Sag, Jiyang Depression, Bohai Bay Basin[J]. Petroleum Exploration and Development, 2014, 41(6): 641-649.

[27]

LI Zheng, WANG Xiuhong, ZHU Rifang, et al. Geochemical evaluation of shale oil in Lower Es3 and Upper Es4 in Jiyang Depression[J]. Xinjiang Petroleum Geology, 2015, 36(5): 510-514.

[28]

ZHANG Pengfei, LU Shuangfang, LI Junqian, et al. Identification method of sweet spot zone in lacustrine shale oil reservoir and its application: A case study of the Shahejie Formation in Dongying Sag, Bohai Bay Basin[J]. Oil & Gas Geology, 2019, 40(6): 1339-1350.

[29]

LI Qianwen, LIU Zhongbao, CHEN Feiran, et al. Lithofacies types and reservoir characteristics of Jurassic shale in the Sichuan Basin revealed by the Da’anzhai Member, Well Y2, Yuanba area[J]. Oil & Gas Geology, 2022, 43(5): 1127-1140.

[30]

XUE Haitao, DING Guozhi, DONG Zhentao, et al. Study on the wettability and spontaneous imbibition characteristics of lacustrine shale[J]. Geofluids, 2022, 4023435.

[31]
DONG Zhentao. Research and application of wettability of shale oil reservoirs in the northern Songliao Basin[D]. Qingdao: China University of Petroleum (East China), 2020.
[32]

HANDY L L. Determination of effective capillary pressures for porous media from imbibition data[J]. Transactions of the AIME, 1960, 219(1): 75-80.

[33]

EWING R P, HORTON R. Diffusion in sparsely connected pore spaces: Temporal and spatial scaling[J]. Water Resources Research, 2002, 38(12): 1285.

[34]

GAO Zhiye, FAN Yupeng, HU Qinhong, et al. Differential development characteristics of organic matter pores and their impact on reservoir space of Longmaxi Formation shale from the south Sichuan Basin[J]. Petroleum Science Bulletin, 2020, 5(1): 1-16.

[35]

ARSALAN N, PALAYANGODA S S, BURNETT D J, et al. Surface energy characterization of sandstone rocks[J]. Journal of Physics and Chemistry of Solids, 2013, 74(8): 1069-1077.

[36]

WANG Yefei, XU Huaimin, QI Ziyuan, et al. Effects of crude fractions on quartz surface wettability and characterization method[J]. Journal of China University of Petroleum (Edition of Natural Science), 2012, 36(5): 155-159.

[37]

ZHANG Hui, WANG Zhizhang, YANG Liang, et al. Quantitative evaluation of shale oil in different occurrence states in first member of Qingshankou Formation of Upper Cretaceous in south of Songliao Basin[J]. Journal of Jilin University (Earth Science Edition), 2022, 52(2): 315-327.

[38]

XI Kelai, ZHANG Yuanyuan, CAO Yingchang, et al. Control of micro-wettability of pore-throat on shale oil occurrence: A case study of laminated shale of Permian Lucaogou Formation in Jimusar Sag, Junggar Basin, NW China[J]. Petroleum Exploration and Development, 2023, 50(2): 297-308.

[39]

LIU Peng, ZHANG Lei, WANG Shengkui, et al. Discussion on migration path of Paleogene shale oil in Jiyang Depression and its petroleum geological significance[J]. Journal of China University of Petroleum (Edition of Natural Science), 2022, 46(6): 89-98.

Oil & Gas Geology
Pages 1142-1154
Cite this article:
LI Q. Wettability and its major determinants of shale reservoirs in the Shahejie Formation, Dongying Sag, Bohai Bay Basin. Oil & Gas Geology, 2024, 45(4): 1142-1154. https://doi.org/10.11743/ogg20240417
Metrics & Citations  
Article History
Copyright
Return