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Research Article | Open Access

The preparation and performance analysis of zirconium-modified aluminum phosphate-based high-temperature (RT–1500 °C) resistant adhesive for joining alumina in extreme environment

Jingxuan Liu1,Yange Wan2,Bo Xiao3Jiancun Li1Zhanming Hu1Ruoyu Zhang4Xiaoxia Hu5Jiachen Liu5Guoshuai Cai2Hongli Liu4( )Mingchao Wang1( )
College of Science, Civil Aviation University of China, Tianjin 300300, China
Department of Safety Engineering, Civil Aviation University of China, Tianjin 300300, China
Binzhou Beicheng Construction Engineering Materials Testing Co., Ltd., Binzhou 256602, China
Department of Aviation Engineering, Civil Aviation University of China, Tianjin 300300, China
School of Materials and Engineering, Key Lab of Advanced Ceramics and Machining Technology of Ministry of Education, Tianjin University, Tianjin 300072, China

Jingxuan Liu and Yange Wan contributed equally to this work.

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Abstract

High-temperature-resistant adhesives are critical materials in the aerospace field. The zirconium-modified aluminum phosphate-based adhesives developed in this work had the advantage of adjustable thermal expansibility, achieving a high matching of coefficient of thermal expansion (CTE) with alumina. The introduction of zirconium can significantly improve the thermal stability of the adhesive matrix, and the Zr/Al ratio substantially affects the various reaction processes inside the adhesive, especially the types of zirconium-containing compounds. Most of the zirconium-containing compounds in the A7Z3 adhesive were ZrO2 only when the mass ratio of zirconium hydroxide to aluminum hydroxide was 3 : 7, which was the key reason why it had the highest CTE. The room-temperature bonding strength of A7Z3 after heat treatment at 1500 °C reached 67.2 MPa. After pretreatment at 1500 °C, the high-temperature bonding strength of A7Z3 was greater than 50 MPa in the range of (room temperature) RT–1000 °C. After 40 thermal cycles between RT and 1500 °C, the bonding strength still reached 10 MPa. Physical bonding occurred at temperatures below 1000 °C, while chemical bonding dominated above 1000 °C based on the generation of Al5BO9 and mullite at the interfaces.

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Journal of Advanced Ceramics
Pages 911-932
Cite this article:
Liu J, Wan Y, Xiao B, et al. The preparation and performance analysis of zirconium-modified aluminum phosphate-based high-temperature (RT–1500 °C) resistant adhesive for joining alumina in extreme environment. Journal of Advanced Ceramics, 2024, 13(7): 911-932. https://doi.org/10.26599/JAC.2024.9220906

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Received: 17 January 2024
Revised: 30 April 2024
Accepted: 01 May 2024
Published: 30 July 2024
© The Author(s) 2024.

This is an open access article under the terms of the Creative Commons Attribution 4.0 International License (CC BY 4.0, http://creativecommons.org/licenses/by/4.0/).

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