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Original Article | Open Access

Comparable Characterization of Nanocellulose Extracted from Bleached Softwood and Hardwood Pulps

Bin Li1,2( ), WenYang Xu2, Dennis Kronlund3, Jan-Erik Eriksson4, Anni Määttänen3, Stefan Willför2, ChunLin Xu2( )
CAS Key Laboratory of Bio-based Materials, CAS Key Laboratory of Biofuels, Qingdao Institute of Bioenergy and Bioprocess Technology, Chinese Academy of Sciences, Qingdao, Shandong Province, 266101, China
Johan Gadolin Process Centre, c/o Laboratory of Wood and Paper Chemistry, Åbo Akademi University, Turku, FI-20500, Finland
Laboratory of Physical Chemistry, Åbo Akademi University, Turku, FI-20500, Finland
Johan Gadolin Process Centre, c/o Laboratory of Inorganic Chemistry, Åbo Akademi University, Turku, FI-20500, Finland
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Abstract

In this study, the characteristics of nanocellulose extracted from bleached softwood and hardwood pulps by formic acid hydrolysis followed by TEMPO-mediated oxidation were compared using transmission electron microscopy (TEM), atomic force microscopy (AFM), Fourier transform infrared analysis (FT-IR), X-ray diffraction (XRD), and thermal gravimetric analysis (TGA). The experimental results showed that the nanocellulose products derived from spruce pulp exhibited a relatively larger particle size, higher crystallinity, and higher thermal stability, compared with the corresponding products obtained from aspen pulp under the same conditions.Furthermore, the study helped establish that the properties of the nanocellulose products were highly dependent on the nature of the starting materials under identical processing conditions.

Keywords

formic acidcomparisonnanocellulosecellulose nanofibrilcellulose nanocrystalTEMPO-mediated oxidation

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Paper and Biomaterials
Volume 3 Issue 4,
October 2018
Pages 35-44
DOI: 10.26599/PBM.2018.9260026
Cite this article:
Li B, Xu W, Kronlund D, et al. Comparable Characterization of Nanocellulose Extracted from Bleached Softwood and Hardwood Pulps. Paper and Biomaterials, 2018, 3(4): 35-44. https://doi.org/10.26599/PBM.2018.9260026

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Received: 25 July 2018
Accepted: 04 September 2018
Published: 01 October 2018
© 2018 Paper and Biomaterials Editorial Board

This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/)
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