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Research Article | Open Access

Effect of High Pressure Homogenization Treatment on Structure and Properties of Soybean Residue Cellulose Nanofibers

Peiyi Li1,2,4,5( ), Yumeng Wang1, Binyao Zhou3, Qingqing Hou1, Hezhen Liu1, Haozhe Lei1, Boxing Jian1, Xinping Li1,4,5
College of Bioresources Chemical and Materials Engineering, National Demonstration Center for Experimental Light Chemistry Engineering Education, Shaanxi University of Science and Technology, Xi'an, Shaanxi Province, 710021, China
State Key Laboratory of Pulp and Paper Engineering, South China University of Technology, Guangzhou, Guangdong Province, 510640, China
Department of Chemical and Paper Engineering, Western Michigan University, Kalamazoo, Michigan, 49008, USA
Key Laboratory of Paper Based Functional Materials of China National Light Industry, Xi'an, Shaanxi Province, 710021, China
Shaanxi Provincial Key Laboratory of Papermaking Technology and Specialty Paper Development, Xi'an, Shaanxi Province, 710021, China
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Abstract

To reduce the adverse effects of non-cellulose materials on subsequent homogenization, the effects of a high-pressure homogenization treatment on the structure and properties of cellulose nanofibers (CNF) prepared by acid treatment of soybean residue were studied. The effects of the number of homogenization step on the microfibrillation degree, crystalline structure and mechanical properties of the soybean residue were analyzed by SEM, FT-IR, XRD, TG and DTG. The results showed that an increase in the number of homogenization steps led to an increase in the degree of microfibrillation, a more uniform distribution of the CNF diameter, and an increase in the crystallinity of CNF. However, but when the number of homogenization steps exceeded 15, the rate of change decreased, and the crystallinity of CNF decreased. As the number of homogenization steps increased, the average degree of polymerization and average molecular weight of CNF decreased continuously, and after 15 homogenization steps, their rate of change also decreased. Therefore, 15 steps of high-pressure homogenization represented a suitable number of steps to prepare the soybean residue CNF with an average diameter of 15 nm.

Keywords

soybean residuecellulose nanofibershigh pressure homogenizationcharacteristics

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Paper and Biomaterials
Volume 4 Issue 4,
October 2019
Pages 37-44
DOI: 10.26599/PBM.2019.9260028
Cite this article:
Li P, Wang Y, Zhou B, et al. Effect of High Pressure Homogenization Treatment on Structure and Properties of Soybean Residue Cellulose Nanofibers. Paper and Biomaterials, 2019, 4(4): 37-44. https://doi.org/10.26599/PBM.2019.9260028

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Received: 12 May 2019
Accepted: 12 July 2019
Published: 01 October 2019
© 2019 Paper and Biomaterials Editorial Board

This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/)
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