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Research Article | Open Access

One-Step Biosynthesis of Gold Nanoparticles Using Natural Reductive Extracts

Ibraheem Jaleel Ibraheem1, Khalil Thabit Hassan2( ), Hameed Hussein Ali1, Ahmed Salman Obaid2
Department of Chemistry, College of Science, University Of Anbar, Ramadi 30001, Iraq
Department of Physics, College of Science, University Of Anbar, Ramadi 30001, Iraq 0000-0002-2902-6998
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Abstract

The green chemical synthesis of nanoparticles was extensively employed in the promotion of the fabrication of nanoparticles. In the present work, a single-step biosynthetic eco-friendly method was utilised to synthesise Au NPs using leave aqueous extracts of Piper nigrum (PN), Ziziphus spina-christi (ZSC), and Eucalyptus globulus (EUCGLO). The extract played the role of the reducing and capping agents where the volume ratios of aqueous extract (100 ppm) to the aqueous solution of HAuCl4·4H2O (0.001 M) were 1:10, 2:10 and 3:10 for all extracts. X-ray powder diffraction (XRD), field emission scanning electron microscopy (FESEM), and ultraviolet-visible spectroscopy (UV-Vis) were performed to characterise the nanoparticles. The surface Plasmon resonance was located at 530, 540, and 533 ± 2 nm for the synthesised Au NPs using the aqueous extract of PN, ZSC, and EUCGLO, respectively. The intensive peaks of XRD patterns indicated the crystalline nature (fcc structure) of the synthesised gold nanoparticles with an average size of 21 ~ 40 nm. The morphology of the Au NPs was carried out by FESEM. The results showed a decline in the spherical shape of the synthesised Au NPs with a mean diameter ranged from 23.7 ~ 33.7 ± 2 nm.

Keywords

Piper nigrum (PN)Ziziphus spina-christi (ZSC)Eucalyptus globulus (EUCGLO)gold nanoparticles (Au NPs)

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Nano Biomedicine and Engineering
Volume 12 Issue 4,
December 2020
Pages 331-337
DOI: 10.5101/nbe.v12i4.p331-337
Cite this article:
Ibraheem IJ, Hassan KT, Ali HH, et al. One-Step Biosynthesis of Gold Nanoparticles Using Natural Reductive Extracts. Nano Biomedicine and Engineering, 2020, 12(4): 331-337. https://doi.org/10.5101/nbe.v12i4.p331-337

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Received: 16 May 2020
Accepted: 13 August 2020
Published: 25 November 2020
© Ibraheem Jaleel Ibraheem, Khalil Thabit Hassan, Hameed Hussein Ali, and Ahmed Salman Obaid.

This is an open-access article distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited.
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