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Article | Open Access

Synthesis and Characterisation of Copper Ⅱ Hydroxide Nano Particles

Post Graduate Department of physics, V.V.Vanniaperumal College for Women, Virudhunagar
Center for Research and Post Graduate Department of Physics, Ayya Nadar Janaki Ammal College, Sivakasi
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Abstract

Copper (Ⅱ) Hydroxide nano particles were synthesized via chemical co-precipitation method from Copper Sulphate and Sodium Hydroxide. Structural and compositional properties were characterized by XRD, SEM, FTIR and UV spectroscopy. XRD confirmed the preferential growth of Copper (Ⅱ) Hydroxide nano particles that width is 33.42nm. The SEM image shows the synthesized Copper (Ⅱ) Hydroxide show well crystallized particles with plate-like morphology. The FTIR spectrum is used to study the stretching and bending frequencies of molecular functional groups in the sample. From UV spectrum, the band gap of Copper (Ⅱ) hydroxide nano particles is found to be 4.5 eV. From AAS studies, it is found that the absorbance is directly proportional to the concentration. The linear fit indicates that Copper (Ⅱ) Hydroxide nanoparticles have been distributed in proper proportion.

References

1

Nasirian A, Synthesis and characterization of Cu nanoparticles and studying of their catalytic properties. Int. J. Nano Dim. 2012; 2: 159-164.

2

Liu X, Geng B, Du Q, Ma J and Liu X, Temperature-controlled self-assembled synthesis of CuO, Cu2O and Cu nanoparticles through a single-precursor route. Material science and engineering A. 2007; 448: 7-14.

3

Sun S, Murry C B, Weller D, Folks L and Moster A, On the synergistic coupling properties of composite CdS / TiO2 nano particle arrays confined in nano patterned hybrid thin films. Science. 2000; 287: 1989.

4

Wang J F, Gudiksen M S, Duan X F and Cui Lieber Y C M. Highly Polarized Photoluminescence and Photo detection from Single Indium Phosphide Nano wires. Science. 2001; 293: 1455.

5

Yu W D and Vivian W Y, Controlled Synthesis of Mono disperse Silver Nano cubes in Water. J. Am. Chem. Soc. 2004; 126: 13200.

6

Petit C, Taleb A and Pileni M P, Self -Organization of Magnetic Nanosized Cobalt Particles. Adv. Mater. 1998; 10: 259.

7

Taleb A, Petit C and Pileni M P, Optical Properties of self assembled 2D and 3D Superlattices of Silver Nanoparticles. Phys. Chem. 1998; 102: 2214.

8

Green M and Brien P O A, simple one phase preparation of organically capped gold nanocrystals. Chem. Commun. 2000; 183.

9

Puntes V F, Zanchet D, Erdonmez C K and Alivisatos A P, Synthesis of hcp-Co Nanodisks. J. Am. Chem. Soc. 2002; 124: 12874.

10

Cordente N, Respaud M, Senocq F, Casanove M J, Amiens C and Chaudret B, Synthesis and Magnetic Properties of Nickel Nanorods. Nanoletters. 2001; 1: 565.

11

Hyeon T, Lee S S, Park J, Chung K and Na H B, Synthesis of Highly Crystalline and Monodisperse Maghemite Nanocrystallites without a Size-Selection Process. J. Am. Chem. Soc. 2001; 123: 12798.

12

Sun S H and Zeng H, Size-Controlled Synthesis of Magnetite nanoparticles. J. Am.Chem. Soc. 2002; 124: 8204.

13

Spencer M S and Twigg M V, Metal Catalyst Design and Preparation in Control of Deactivation. Annu. Rev. Mater. Res. 2005; 35: 427.

14

Masala O and Seshadri R, Synthesis routes for large volumes of nanoparticles. Annu. Rev. Mater. Res. 2004; 34: 41–81.

15

Zhang H, Dong X, Lin G, Liang X and Li H, Carbon nanotubepromoted Co–Cu catalyst for highly efficient synthesis of higher alcohols from syngas. Chem. Commun. 2005; 5094.

16

Bettge M, Chatterjee J and Haik Y, Physically synthesized Ni-Cu nanoparticles for magnetic hyperthermia. Biomagnetic Res. Tech. 2004; 2: 4.

17

Jiang H, Moon K, Lu J and Wong C, Conductivity enhancement of nano silver-filled conductive adhesives by particle surface functionalization. J. Elect. Mat. 2005; 34: 1432.

18

Narayan J and Nanopart, Preparation of carbon-coated Co and Ni nanocrystallites by a modified AC arc discharge method. Materials science and engineering B. 2000; 100: 186-190.

19

Pileni M P, Ninham B W, Krzywicki T G, Tanori J, Lisiecki I and Filankembo A, Direct Relationship Between Shape and Size of Template and Synthesis of Copper Metal Particles. Adv. Mater. 1999; 11: 1358.

20

Han W, Choi J, Hwang G, Hong S, Lee J and Kang S, Fabrication of Cu nano particles by direct electrochemical reduction from CuO nano particles. Appl. Surf. Sci. 2006; 252: 2832.

21

Ohde H, Hunt F, Wai C M, Synthesis of Silver and Copper nano particles in a water-in-supercritical-carbon dioxide microemulsion. Chem. Mater. 2001; 13: 4130.

22

Samin M, Kaushik N K and Maitra Bull, A Effect of size of copper nanoparticles on its catalytic behaviour in Ullman reaction. Mater. Sci. 2007; 30: 535-540.

23

Ponce A N A and Klabunde K J, Chemical and catalytic activity of copper nanoparticles prepared via metal vapor synthesis. J. Molecular catalysis A: Chemical. 2005; 255: 1-6.

24

Hassan J, Penalva V, Lavenot L, Gozzi C and Lemaire M, Catalytic alternative of the Ullmann reaction. J. Tetrahedron. 1998; 54: 13793-13840.

25

Rathi R K, Subramanian S, Sivanandam V and Pradeep T, Studies on the interaction of Guar gum with Chalcopyrite. Canadian Metallurgical Quarterly. 2001; 40: 01-12.

26
Gadsden J A, Infrared Spectra of Minerals and Related Inorganic Compound Butterworths U K. 1975.
27

Jhon Mauricio Aguirre A D, Adamo Gutiérrezb D and Oscar iraldo C D, Simple Route for the Synthesis of Copper Hydroxy Salts. J. Braz. Chem. Soc. 2011; 22: 546-551.

28

Henrist C, Traina K Hubert, Toussaint G Rulmont A and Cloots R, Study of the morphology of copper hydroxynitrate nanoplatelets obtained by controlled double jet precipitation and urea hydrolysis. J. Cryst. Growth. 2003; 254: 176-187.

29

Frost R L and Kloprogge J T, Infrared emission spectroscopic study of brucite. Spectrochim. Acta Part A. 1999; 55: 2195-2205.

30

Theivasanthi T and Alagar M, Konjac Biomolecules Assisted–Rod/Spherical Shaped Lead Nano Powder Synthesized by Electrolytic Process and Its Characterization Studies. Nano Biomed. Eng. 2013; 5(1): 11-19

Nano Biomedicine and Engineering
Pages 116-120
Cite this article:
Devamani RHP, Alagar M. Synthesis and Characterisation of Copper Ⅱ Hydroxide Nano Particles. Nano Biomedicine and Engineering, 2013, 5(3): 116-120. https://doi.org/10.5101/nbe.v5i3.p116-120
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